- Разработка метода высокоскоростной дифрактометрии и малоуглового рентгеновского рассеяния синхротронного излучения для исследования быстропротекающих твердофазных реакций с параметрами: экспозиция от 1 нс, периодичность от 125 нс.
- Реальная структура деформированных металлов: серебра, меди и никеля через 0,4 с после среза. Параметры релаксационных процессов в этих металлах в первые секунды после деформации на воздухе и при контакте с электролитами.
- Структура кристаллической решетки никеля во время электрохимического наводораживания. Структура кристаллической решетки гидрида никеля с момента образования зародышей до развития устойчивой фазы при нескольких циклах гидрирования - дегидрирования.
- Двухстадийный механизм твердофазного синтеза молибдата никеля из NiO и MoO3 через образование твердого раствора g-Мо4011/NiO. Нестабильность кислородного октаэдрического окружения никеля при росте температуры выше 650 oС - причина разрушения b-NiМоO4 при высоких температурах.
- Кинетика твердофазного синтеза вольфрамата никеля из NiO и WO3 при температурах выше и ниже 720 oС. Структурные параметры зародышей новой фазы NiWO4 в первые секунды реакции и их зависимость от температуры.
- Условия образования монодисперсных наночастиц серебра при термическом разложении его карбоксилатов CnH2n-1O2Ag (n = 6, 8, 10, 12, 14, 16, 18, 22) и формирования упорядоченных периодических структур. Кристаллическая структура образовавшегося трехмерного коллоидного кристалла. Диапазоны устойчивого существования упорядоченных наноструктур.
- Структура интерметаллида толщиной 20-50 нм, образующегося при холодном газодинамическом напылении мелкодисперсных частиц алюминия на подложку из никеля.
- Структура продуктов фазового перехода адамантана при его нагружении ударной волной и условия синтеза наночастиц металлов: серебра, никеля, кобальта при ударно-волновом воздействии на стеараты серебра, никеля, кобальта, висмута и свинца, соответственно.
- Метод удержания реагентов в экстремальных условиях (большие температуры и давления) и, как следствие, управление скоростью зародышеобразования наноалмазов. Метод обеспечен возможностью диагностического зондирования объекта исследования пучком синхротронного излучения и получения структурной информации о наноалмазах.
2. A.N. Aleshaev, M.G. Fedotov, G.N. Kulipanov, N.Z. Lyakhov, L.A. Luk’yanchikov, S.I. Mishnev, M.A. Sheromov, K.A. Ten, V.M. Titov, B.P. Tolochko, P.I. Zubkov. Synchrotron radiation instrumentation for "in situ" investigation of explosion with nanosecond time resolution.// Nuclear Instruments and Methods in Physics Research Section A, Volume 467-468, Part 2, 2001, p. 990- 993.
3. A.N. Aleshaev, O.V.Evdokov, M.G. Fedotov, G.N. Kulipanov, N.Z. Lyakhov, L.A. Luk’yanchikov, S.I. Mishnev, M.A. Sheromov, K.A. Ten, V.M. Titov, B.P. Tolochko, P.I. Zubkov. Methods of research of the detonation and shock wave processes with the help of SR. Possibilities and prospects.// Nuclear Instruments and Methods in Physics Research, A470, 2001. p. 240-244.
4. A.N.Aleshaev, M.G.Fedotov, N.G.Gavrilov, S.I.Mishnev, V.E.Panchenko, V.F.Pindyurin, I.V.Poletaev, B.P.Tolochko. Stabilization system of synchrotron radiation beams at the VEPP-3 storage ring.// Nuclear Instruments and Methods in Physics Research, A470, 2001. pp. 94-100.
5. A.V. Bolesta, V.M. Fomin, M.R. Sharafutdinov, B.P. Tolochko. Investigation of interface boundary occuring during cold gas-dynamic spraying of metallic particles.// Nuclear Instruments 35 and Methods in Physics Research, A 470 (2001), p.249.
6. A.V.Bessergenev, A.M.Fogg, R.J.Frances, S.J.Price, D.O’Hare, V.P.Isupov, B.P.Tolochko. Synthesis and Structure of the Gibbsite Intercalation Compounds [LiAl2(OH)6]X {x = Cl, Br, NO3} and [LiAl2(OH)6]Cl.H2O using Synchrotron X-ray and Neutron Powder Diffraction.// American Chemical Society Journal, Chemistry of Materials -1997, v.9, p. 241-247.
7. A.V.Bessergenev, B.P.Tolochko. Simultaneous two energies anomalous scattering for the study of the dynamics of structural transformation.// Nuclear Instruments and Methods in Physics Research, A 359, 1995 p 160-164.
8. Aulchenko V. Bukin M. Gaponenko I. Titov V, B.P.Tolochko. The Data Acquisition and On-line Visualisation System for the OD-3 Fast One-Coordinate Detector.// Nuclear Instruments and Methods, 1998, Volume A405, p. 163-167.
9. Aulchenko V., O. Evdokov, S. Ponomarev, L. Shekhtman, K. Ten, B. Tolochko, I. Zhogin, V. Zhulanov. Development of fast one-dimensional X-ray detector for imaging of explosions.// Nuclear Instruments and Methods in Physics Research. Section A: 2003, v. 513, N 1-2, p. 388- 393.
10. B.P. Tolochko, V.M. Titov, A.P. Chernyshev, K.A. Ten, E.R. Pruuel, I.L. Zhogin, P.I. Zubkov, N.Z. Lyakhov, L.A. Lukyanchikov Physical–chemical model of processes at detonation synthesis of nanodiamonds.// Diamond and Related Materials, – 2007, 16, p. 2014–2017.
11. B.P.Tolochko, S.G.Nikitenko, A.N.Aleshaev, G.N.Kulipanov, S.I.Mishnev XANES Registration by Electron Beam Position Scanning for Time-Resolved Experiment.// J. DE PHYSIQUE IV, (Supplement au Journal de Physique III, №.4), Vol. 7, 1997, p. C2-549-552.
12. B.P.Tolochko, S.V. Chernov, S.G.Nikitenko The "In Situ" Research of the Synthesis of NiMoO4 J. DE PHYSIQUE IV, (Supplement au Journal de Physique III, №.4), Vol. 7, 1997, p. C2 961- 964.
13. Bokhonov B. B., A. A. Sidelnikov, M. R. Sharafutdinov, B. P. Tolochko, L. P. Burleva, D. R. Whitcomb. Thermal and mechanochemical initiated phase transformations in silver carboxylates.// Journal of Imaging Science and Technology - 2003, v. 47, N 2, р. 89-99.
14. Bokhonov B. B., Sharafutdinov M. R., Tolochko B. P., Burleva L. P., Whitcomb D. R. In situ Xray investigation of metallic silver phase formation from silver myristate thermal decomposition and from its reduction in photothermographic films.// Journal of Imaging Science and Technology, 2005, vol. 49, N 4, p. 389-393.
15. Bokhonov B.B., Sharafutdinov M.R., Tolochko B.P., Burleva L.P., Whitcomb D. R. In situ X-ray investigation of the formation of metallic silver phases during the thermal decomposition of silver behenate and thermal development of photothermographic films // Journal of Imaging Science and 36 Technology. - 2007. - V. 51. -№ 4. -P. 385-390.
16. Chernyshev A.P., Lukyanchikov L.A., Lyakhov N.Z., Pruuel E.R., Sheromov M.A., Ten K.A., Titov V.M., Tolochko B.P., Zhogin I.L., Zubkov P.I. Physical-chemical model of nanodiamond formation at explosion // Nuclear Instruments and Methods in Physics Research. Sec. A. – 2007. – Vol. 575, No 1/2. – P. 72-74.
17. E.A. Babichev, S.E. Baru, V.R. Groshev, A.G. Khabakhpashev, G.M. Kolachev, V.V. Porosev, G.A. Savinov, A.I. Ancharov, B.J. Pirogov, M.R. Sharafutdinov, B.P. Tolochko. The position sentensive 1D-160 detector for high resolution powder diffraction.// Nuclear Instruments and Methods in Physics Research, A 470 (2001), p.173
18. E.Yu.Belyaev, O.I.Lomovsky, A.I.Ancharov, B.P.Tolochko Investigation of the reaction zone structure under mechanochemical synthesis of metal disilicides by a method of local diffractometry.// Nuclear Instruments and Methods, 1998, Volume A405 435-439
19. F.Neissendorfer, H.J.Rossa, K.P.Thiessen, B.P.Tolochko, S.V.Mytnichenko, M.A.Sheromov, Xray stress measurements with synchrotron radiation.// Nuclear Instruments and Methods in Physics Research 1991,V. A308, 1/2. р. 276-277
20. F.Nessendorfer, U.Steinike, M.A.Sheromov, B.P.Tolochko On the decomposition of hydrargillite investigated by synchrotron X-ray diffraction.// Nuclear instruments and methods in phisics research. Sec. A., 1987, v.A261, № 1/2 p.219-220
21. F.Nessendorfer, U.Steinike, M.A.Sheromov, B.P.Tolochko Crystalization of amorthous aluminium phosphate investigated by sinchrotron X-ray diffraction.// Nuclear instruments and methods in phisics research. Sec. A., 1987, v.A261, № Ѕ p.216-218
22. G.M. Rylov , E.S.Yefimova, N.V.Sobolev, G.N. Kulipanov, V.I. Kondratyev, B.P. Tolochko, M.R. Sharafutdinov. Study of imperfect natural diamonds with the application of the X-ray synchrotron radiation (the “Laue-SR” method). // Nuclear Instruments and Methods in Physics Research, A 470 (2001), p.182
23. K.A. Tarasov, V.P. Isupov, B.B. Bokhonov, Yu.A. Gaponov, B.P. Tolochko, M.M. Yulikov, V.F. Yudanov, A. Davidson, P. Beaunier, E. Marceau, M. Che. Control of particle size via chemical composition: Structural and magnetic characterization of Ni–Co alloy nanoparticles encapsulated in lamellar mixed oxides.// Microporous and Mesoporous Materials 107 (2008) 202–211.
24. Kondratyev V.I., Kuzin M.V., Mezentsev N.A., Mezentseva L.A., Nazmov V.P., Pavlyukhin Yu.T., Pindyurin V.F., Sidelnikov A.A., Tolochko B.P. Preliminary testing of microstructured Imaging Plates with improved spatial resolution.// Nuclear instruments and methods in physics research. Sec. A. – 2000. - Vol. A448, No 1/2. – P. 207-210.
25. Korneev V.N., Sergienko P.M., V.A.Shlektarev, Aulchenko V.M., Titov V.M., Tolochko B.P., 37 Sharafutdinov M.R., Zabelin A.V., Najda O.V., Vazina A.A. New time-resolved small-angle station with the use of synchrotron radiation of the Siberia-2 storage ring for investigation of biological structures.// J.Glass Physics and Chemistry. 2007. V. 33, no. 3, p. 266-270.
26. M.G. Fedotov, G.N. Kulipanov, N.Z. Lyakhov, L.A. Luk’yanchikov, M.R. Sharafutdinov, M.A. Sheromov, K.A. Ten, V.M. Titov, B.P. Tolochko, P.I. Zubkov. Dynmamics of formation of particles of the condensed carbon phase at shock compression of organic materials.// Nuclear Instruments and Methods in Physics Research Section A, Volume 470, Part 2, 2001, pp. 245-248.
27. M.R. Sharafutdinov, B.P. Tolochko, N.Z. Lyakhov. Usage of synchrotron radiation diffraction for “in situ” kinetic study of nickel tungstenate solid state synthesis. // Nuclear Instruments and Methods in Physics Research, A 470 (2001), p.228.
28. Merzhievsky L.A., Lukianchikov L.A., Pruuel E.R., Ten K.A., Titov V.M., Tolochko B.P., Evdokov O.V., Zhogin I.L., Sheromov M.A. Synchrotron diagnostics of shock-wave compression of aerogel.// Nuclear instruments and methods in physics research. Sec. A. – 2007. – Vol. 575, No 1/2. – P. 121-125.
29. Michnev S.I., Aleshaev A.N., FedotovM.G., Tolochko B.P. “Moving source”: test realization at VEPP-3 of a diffraction experiment with nanosecond time resolution // Nuclear instruments and methods in physics research. Sec. A. – 2000. - Vol. A448, No 1/2. – P. 234-240. – Bibliogr.: 3 ref.
30. N.A.Mezenzev, B.P.Tolochko. Experimental station for the study of the dynamics of the structural changes using synchrotron radiation.// Nuclear Instruments and Methods, 1986, V.A246, № 1/3 P.604-608
31. N.Lyakhov, Yu.Gaponov, B.P.Tolochko Use of synchrotron radiation for studyng the mechanism of solid state reactions Solid State Ionics, 1997, v. 101-103 1251-1256
32. N.Z.Lyakhov, A.I.Maslii, M.A.Sheromov, B.P.Tolochko Investigation of the dynamics of relaxation processes in silver deformed by a cut.// Nuclear instruments and methods in phisics research. Sec. A., 1987, v.A261, № 1/2 p.209-215
33. O.V.Evdokov, M.G. Fedotov, G.N. Kulipanov, N.Z. Lyakhov, L.A. Luk’yanchikov, M.R. Sharafutdinov, M.A. Sheromov, K.A. Ten, V.M. Titov, B.P. Tolochko, P.I. Zubkov Dynamics of the formation of the condensed phase particles at detonation of high explosives.// Nuclear Instruments and Methods in Physics Research Section A, Volume 470, Part 2, 2001, pp. 236-239.
34. Rogachev A.S., Gachon J.-C., Grigoryan H.E., Illekova E., Kochetov N.F., Nosyrev F.N., Sachkova N.V., Schuster J.C., Sharafutdinov M.R., Shkodich N.F., Tolochko B.P., Tsygankov P.A., Yagubova I.Y. Diffraction of synchrotron radiation for in situ study of the heterogeneous reaction mechanisms in lamellar composites obtained by mechanical activation and magnetron sputtering // Nuclear instruments and methods in physics research. Sec. A. – 2007. – Vol. 575, No 38 1/2. – P. 126-129. – Bibliogr.: 11 ref.
35. S.V.Chernov, S.G.Nikitenko, D.R.Whitcomb, B.P.Tolochko Determination of the crystal structure of silver stearate and its temperature changes by Ag K-EXAFS spectroscopy. Nuclear Instruments and Methods, 1998, Volume A405 428-434
36. Sharafutdinov M.R., Korchagin M.A., Shkodich N.F., Tolochko B.P., Tsygankov P.A., Yagubova I.Yu. Phases transformations in the Ni-Al system investigation by synchrotron radiation diffraction // Nuclear instruments and methods in physics research. Sec. A. – 2007. – Vol. 575, No 1/2. – P. 149-151. – Bibliogr.: 9 ref.
37. Ten K.A., O.V. Evdokov, I.L. Zhogin, V.V. Zhulanov, P.I. Zubkov, G.N. Kulipanov, L.A. Luk’yanchikov, L.A. Merzhievsky, B.Ya. Pirogov, E.R. Pruuel, V.M. Titov, B.P. Tolochko, M.A. Sheromov. Density distribution reconstruction of the detonation front of high explosives using synchrotron radiation data.// Nuclear Instruments and Methods in Physics Research, 2005, vol. A 543, р. 170-174.
38. Tolochko B.P., Kulipanov G.N., Mezentsev N.A., Mishnev S.I. “Moving source”: feasibility of diffraction experiment with nanosecond time resolution by the fast synchrotron radiation beam scanning // Nuclear instruments and methods in physics research. Sec. A. – 2000. - Vol. A448, No 1/2. – P. 228-233. – Bibliogr.: 4 ref.
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40. U.Steinike, H.Krechmar, B.P.Tolochko Structural changes in MgO by treatment in planetar mill.// Crystal Research and Technology, 1983, v.18, n. 6 793-796
41. V.Aulchenko, V. Zhulanov, L. Shekhtman, B. Tolochko, I. Zhogin, O. Evdokov, K. Ten. Onedimensional detector for study of detonation processes with synchrotron radiation beam.// Nuclear Instruments and Methods in Physics Research, 2005, vol. A 543, р. 350-356.
42. V.L.Shapkin, B.P.Tolochko V.V.Boldyrev Experimental study of rapid structural transformation during synthesis of the fluorpatite using synchrotron radiation diffraction.// Nuclear Instruments and Methods, 1998, Volume A405 494-495.
43. V.M. Aulchenko, M.A. Bukin, A.D. Drozdetsky, M.S. Dubrovin, M.R. Sharafutdinov, V.M. Titov, B.P. Tolochko, A.V. Vasiljev, Yu.S. Velikzhanin. Fast parallax-free one-coordinate X-ray detector OD120 with registration angle up to 360 degree.// Nuclear Instruments and Methods in Physics Research, A 470 (2001), p.168.
44. V.M. Aulchenko, O.V. Evdokov, V.D. Kutovenko, B.Ya. Pirogov, M.R. Sharafutdinov, V.M. 39 Titov, B.P. Tolochko, A.V. Vasiljev, I.A. Zhogin, V.V. Zhulanov. One-coordinate X-ray detector OD-3M.// Nuclear Instruments and Methods in Physics Research A 603 – 2009, p. 76-79.
45. V.M. Titov, B.P. Tolochko, K.A. Ten, L.A. Lukyanchikov and E.R. Pruuel. Where and when are nanodiamonds formed under explosion?// Diamond and Related Materials – 2007, 16, p. 2009– 2013.
46. V.M.Aulchenko,A.A.Vazina, V.S.Gerasimov, P.M.Sergienko, M.R.Sharafutdinov V.P.Tolochko. The station for time-resolved investigation in wide and small angles of diffraction.// Nuclear Instruments and Methods - 1998, A405, pp. 487-493
47. V.M.Aul´chenko. A.B.Bessergenev O.A.Evdokov V.S.Gerasimov M.A.Sheromov, B.P.Tolochko A.A.Vazina.The station for time resolved investigation in wide and small anglees diffraction.// Nuclear Instruments and Methods, 1998, Volume A405 139-142
48. V.V.Boldyrev, Yu.A.Gaponov, N.Z.Lyakhov, A.A.Politov, T.P. Shakhtshneider, M.A.Sheromov, B.P.Tolochko Experience in use of synnchrotron radiation in solid state chemistry studies.// Nuclear instruments and methods in phisics research. Sec. A., 1987, v.A261, № 1/2, p.192-199
49. Volosov V.I. Churkin I.N. , B.P.Tolochko X-Ray diffraction of samples irradiated by intensive atomic flows of low energy.// Nuclear Instruments and Methods, 1998, Volume A405, p.171-175.
50. Yu.A.Gaponov, B.P.Tolochko Station for studying solid-state chemical reactions by Laue method.// Review of scientific instruments V.60, № 7, July 1992 p.2429-2432.